期刊
JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY
卷 19, 期 6, 页码 3654-3657出版社
AMER SCIENTIFIC PUBLISHERS
DOI: 10.1166/jnn.2019.16492
关键词
Ferrite; Mechanochemistry; Nanomaterial; Raman Spectroscopy; Mossbauer
类别
资金
- Deutsche Forschungsgemeinschaft [SE 1407/4-1]
- Moravian-Silesian Region
- project RMTVC [LO1203]
- Student Grant Competition [SP2016/94]
Nanostructured nickel ferrite (NiFe2O4) is prepared via high-energy ball milling of the bulk counterpart at ambient temperature. The structure of the as-prepared nanoferrite is characterized by Raman spectroscopy and Fe-57 Mossbauer spectroscopy. Due to the ability of these spectroscopic techniques to probe the local environment of ions, valuable complementary insight into the nature of the local structural disorder of nanosized NiFe2O4, is provided. For the first time, evidence is given of the tetrahedrally coordinated nickel cations in the nanomaterial.
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