期刊
FOOD CHEMISTRY
卷 278, 期 -, 页码 67-76出版社
ELSEVIER SCI LTD
DOI: 10.1016/j.foodchem.2018.11.056
关键词
UHPLC-ESI-Q/Orbitrap; Nutraceutical products; High-throughput screening; Non-target; Green tea
资金
- National Natural Science Foundation of China [31801643]
- Shaanxi Provincial Education Department [17JK0112]
A new multi-analytical strategy was developed to screen mycotoxins and their transformation products in nutraceuticals from green tea. Seven class mycotoxins were determined using a fully automated on-line extraction procedure followed by ultrahigh-performance liquid chromatography coupled to high resolution mass spectrometry. This multi-analytical methodology has been explored providing an entire spectrum of fragment ion peaks for each mycotoxin, which allows unbiased high-throughput screening and quantitation of non-target mycotoxins. The validated mycotoxins exhibited satisfactory recoveries in the range of 82-108% in accordance with 2002/657/EC. The coefficients of linear determination were in the range of 0.9920-0.9999, with relative standard deviations were in the range of 3.2-14.9%. CC beta ranged between 0.022 mu g kg(-1) and 0.50 mu g kg(-1). The screening and confirmation method was applied to green tea nutraceuticals. Seven samples were found to be positive for mycotoxins at concentrations ranging from 0.23 mu g kg(-1) (3-acetyldeoxynivalenol) to 7.92 mu g kg(-1) (T-2 toxin).
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