期刊
CHEMISTRY-A EUROPEAN JOURNAL
卷 25, 期 19, 页码 4931-4934出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/chem.201900009
关键词
Csp(3)-H functionalization; EPR spectroscopy; Ni catalyst; Ni-III species; X-ray absorption spectroscopy
资金
- National Natural Science Foundation of China [21701127, 21762023, 21520102003]
- Hubei Province Natural Science Foundation of China [2017CFB152]
- Natural Science Foundation of Jiangxi Province of China [2018BAB203006]
- Fundamental Research Funds for the Central Universities [213413000050]
- Scientific Research Foundation of Wuhan University [413100043, 413100021]
An in situ generated oxidation species of nickel quinolinylpropioamide intermediate was produced. Characterization by X-ray absorption near edge structure (XANES) and EPR provides complementary insights into this oxidized nickel species. With aliphatic amides and isocyanides as substrates, a nickel-catalyzed facile synthesis of structurally diverse five-membered lactams could be achieved.
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