期刊
CERAMICS INTERNATIONAL
卷 45, 期 13, 页码 16638-16644出版社
ELSEVIER SCI LTD
DOI: 10.1016/j.ceramint.2019.05.205
关键词
VN powders; Molten-salt; Crystal morphology; Performance
资金
- National Natural Science Foundation of China [51502215, 51574187, 51602232]
- Natural Science Foundation of Hubei Province [2018CFA022]
VN powders were synthesized in NZ atmosphere by using V2O5 and Mg as raw materials in KCl-KF molten salt environment. The effects of reaction temperature, reaction time and the presence or absence of salts on the formation of VN powders were investigated. The results showed that when the temperature increased to 700 degrees C, pure phase VN powders were fabricated, along with the specific surface area of 8.428 m(2) g(-1). As the temperature rose from 700 to 800 degrees C, VN powders presented the smallest average size of 0.10 mu m. The electro-chemical performance test showed that the specific capacitance of VN was 25 F/g at 0.5 A/g and the internal resistance was 1.8 Omega. The VN emission peak was composed of 263, 388 and 547 nm, indicating that it has good optical properties. A possible synthesis mechanism of VN powders in molten salt environment powders is proposed.
作者
我是这篇论文的作者
点击您的名字以认领此论文并将其添加到您的个人资料中。
推荐
暂无数据