期刊
RESEARCH ON CHEMICAL INTERMEDIATES
卷 45, 期 5, 页码 2999-3018出版社
SPRINGER
DOI: 10.1007/s11164-019-03775-7
关键词
Mesoporous nanocatalyst; Silica-based nanocatalyst; Nano-N,N,N ',N '-tetramethyl-N-(silica-n-propyl)-N '-sulfo-ethane-1,2-diaminium chloride (nano-[TSPSED][Cl](2)); N,N '-alkylidene bisamide; Solvent-free
资金
- Payame Noor University
A novel mesoporous nanomaterial, namely nano-N,N,N',N'-tetramethyl-N-(silica-n-propyl)-N'-sulfo-ethane-1,2-diaminium chloride (nano-[TSPSED][Cl](2)), was prepared, and characterized using Fourier-transform infrared spectroscopy (FT-IR), energy-dispersive X-ray spectroscopy (EDS), field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM), adsorption/desorption porosimetry (BET, Langmuir, BJH and adsorption/desorption isotherm), thermal gravimetric (TG), differential thermal gravimetric (DTG) and X-ray diffraction (XRD) analyses. Afterward, nano-[TSPSED][Cl](2) was used as a highly efficient and recyclable nanocatalyst for the condensation reaction of primary amides (2 eq.) with arylaldehydes (1 eq.) under solvent-free conditions to afford N,N'-alkylidene bisamides in high yields and in short times.
作者
我是这篇论文的作者
点击您的名字以认领此论文并将其添加到您的个人资料中。
推荐
暂无数据