期刊
MOLECULES
卷 24, 期 5, 页码 -出版社
MDPI
DOI: 10.3390/molecules24050937
关键词
rhodium; annulation; Boc-protected benzamides
资金
- National Natural Science Foundation of China [81620108027, 21632008, 21672231]
- Major Project of Chinese National Programs for Fundamental Research and Development [2015CB910304]
A mild rhodium-catalyzed annulation of Boc-protected benzamides with diazo compounds via C-C/C-O bond formation has been explored. In the presence of [Cp*RhCl2](2), AgSbF6 and Cs2CO3, Boc-protected benzamides can be effectively annulated to yield isocoumarins in 0.5-2 h.
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