期刊
ANALYTICAL AND BIOANALYTICAL CHEMISTRY
卷 408, 期 19, 页码 5053-5074出版社
SPRINGER HEIDELBERG
DOI: 10.1007/s00216-016-9676-8
关键词
Single particle ICP-MS; ICP-TOF-MS; Engineered nanoparticles; Environmental analysis; Core-shell nanoparticles; FFF-ICP-MS
资金
- National Science Foundation [CBET-1336168, CBET-1512695]
- Environmental Protection Agency [RD83558001]
- Center for the Environmental Implications of Nanotechnology
- Directorate For Engineering
- Div Of Chem, Bioeng, Env, & Transp Sys [1336168] Funding Source: National Science Foundation
- Div Of Chem, Bioeng, Env, & Transp Sys
- Directorate For Engineering [1512695] Funding Source: National Science Foundation
From its early beginnings in characterizing aerosol particles to its recent applications for investigating natural waters and waste streams, single particle inductively coupled plasma-mass spectrometry (spICP-MS) has proven to be a powerful technique for the detection and characterization of aqueous dispersions of metal-containing nanomaterials. Combining the high-throughput of an ensemble technique with the specificity of a single particle counting technique and the elemental specificity of ICP-MS, spICP-MS is capable of rapidly providing researchers with information pertaining to size, size distribution, particle number concentration, and major elemental composition with minimal sample perturbation. Recently, advances in data acquisition, signal processing, and the implementation of alternative mass analyzers (e.g., time-of-flight) has resulted in a wider breadth of particle analyses and made significant progress toward overcoming many of the challenges in the quantitative analysis of nanoparticles. This review provides an overview of spICP-MS development from a niche technique to application for routine analysis, a discussion of the key issues for quantitative analysis, and examples of its further advancement for analysis of increasingly complex environmental and biological samples.
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