期刊
COMPOSITES PART B-ENGINEERING
卷 160, 期 -, 页码 573-585出版社
ELSEVIER SCI LTD
DOI: 10.1016/j.compositesb.2018.12.055
关键词
Plasma functionalization; Multilayered graphene; Graphene exfoliation; Cement composite; Nanoreinforcement
资金
- University of the Philippines Diliman Office of the Vice-Chancellor for Research and Development Outright Research Grant (OVCRD Project) [141404 PNSE]
- University of the Philippines Diliman Office of the Vice-President for Academic Affairs Balik-PhD Research Grant [OVPAA-BPhD-2014-01]
- Jardiolin Family Professorial Chair
- nanoQuench project (CHED PCARI Project) [IIID 2016-007]
A fast, facile, nonhazardous, environment-friendly, and high yield process was developed for the plasma treatment of graphite particles and the production of plasma-functionalized multilayered graphene (pf-MLG). Graphite particles (< 20 mu m) were functionalized using a subatmospheric 13.56 MHz radio frequency-excited oxygen plasma followed by liquid-phase exfoliation to produce pf-MLG with a high aspect ratio (> 2585) with < 20 graphene layers. The exfoliated graphene also exhibited high dispersibility in water after plasma functionalization without the use of surfactants. The pf-MLG nanoflakes were incorporated into a cement mixture with 0.1 and 0.5 wt% pf-MLG loading. A 56% increase in compressive strength of cement mortars was achieved for the 0.5 wt% pf-MLG after 28 days curing. This is attributed to the strong interfacial interaction between graphene and the cement matrix and the promotion of hydration. The highly scalable process of pf-MLG-reinforced cement will make a positive impact on the environment, especially in the construction industry.
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