期刊
ADVANCED SYNTHESIS & CATALYSIS
卷 358, 期 5, 页码 719-723出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adsc.201501068
关键词
cross dehydrogenative coupling (CDC) reactions; dyes; green chemistry; phosphoramidates; photocatalysis
资金
- International Science & Technology Cooperation Program of China [2014DFE40130]
- European Regional Development Fund (ERDF) [4061]
- EPSRC [EP/K039466/1]
- NRF Nano.Material Technology Development Program [2012M3A7B4049652]
- EU [FP7-MC-CIG-618237]
- Engineering and Physical Sciences Research Council [EP/K039466/1, 1499412] Funding Source: researchfish
- National Research Foundation of Korea [2012M3A7B4049645] Funding Source: Korea Institute of Science & Technology Information (KISTI), National Science & Technology Information Service (NTIS)
- EPSRC [EP/K039466/1] Funding Source: UKRI
We describe the use of visible light in conjunction with an organic dye for the synthesis of phosphoramidates. Cross dehydrogenative coupling reactions between phosphites and amines are reported using organic dyes and light as catalysts for the first time. It is not only a novel application of organic dyes but also fulfils the requirement of sustainability and green chemistry avoiding the use of chromatographic purification techniques. The product was simply isolated from the reaction mixture via an acid-base work-up procedure, rendering the pure product in good yields.
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