期刊
ADVANCED SYNTHESIS & CATALYSIS
卷 358, 期 23, 页码 3840-3846出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adsc.201600700
关键词
alkylamination; C-H functionalization; iron catalysis; phenols; synthetic methods
资金
- National Natural Science Foundation of China [21321061, 21072134, J1103315/J0104]
- Applied Basic Research Foundation of Sichuan Province
A novel iron-catalyzed direct alkylamination reaction of phenols has been achieved with O-benzoyl-N-alkylhydroxylamines as aminating agents. This protocol provides a facile access to N-alkyl-substituted aminophenols though a radical reaction from phenols. The catalytic direct alkylamination operates at room temperature without the need of any ligands and additives to afford the desired products with excellent regioselectivity and functional group tolerance.
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