期刊
ACTA MATERIALIA
卷 107, 期 -, 页码 229-238出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.actamat.2016.01.042
关键词
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资金
- European Union [312483 - ESTEEM2]
- European Research Council under the European Union's Seventh Framework Programme (FP)/ERC grant [291522 - 3DIMAGE]
- Royal Society's Newton International Fellowship
- Rolls-Royce
- EPSRC
- BMWi [EP/H022309/1, EP/H500375/1, 20T0813]
- ERC [259619 PHOTO EM]
- Engineering and Physical Sciences Research Council [EP/M005607/1, 1232071] Funding Source: researchfish
- EPSRC [EP/M005607/1] Funding Source: UKRI
The gamma' strengthening phase in an advanced nickel-based superalloy, ATI 718Plus, was characterized using a blind source separation applied to a four dimensional X-ray microanalysis dataset obtained by scanning transmission electron microscopy. Selected patterns in the X-ray spectra identified by independent component analysis were found to be spatially and chemically representative of the matrix (gamma) and precipitate phases (gamma') present in the superalloy, enabling their size, shape and distribution to be determined. The three dimensional chemical reconstruction of the microstructure may provide insight into the role of the various alloying elements in the evolution of the microstructure at the nano-scale. (C) 2016 Acta Materialia Inc. Published by Elsevier Ltd.
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