期刊
ORGANIC LETTERS
卷 20, 期 21, 页码 6906-6909出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.8b03050
关键词
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资金
- National Science Foundation of China [21572099, 21332005]
- Natural Science Foundation of Jiangsu Province [BK20151379]
- State Key Laboratory Cultivation Base for TCM Quality and Efficacy, Nanjing University of Chinese Medicine [TCMQ, E 201702]
- open training program of the undergraduate organic experiment course [0205145031-6]
The first example of constructing a C-sp3-C-sp bond with substituted Hantzsch ester and Meyer nitrile is reported. When benziodoxole-activated alkyne was applied as the alkynyl donor, products containing C-sp3-C-sp bonds involving primary, secondary, and tertiary carbon centers were achieved in up to 97% yields. K2S2O8 was the optimum radical initiator in this reaction.
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