期刊
ORGANIC LETTERS
卷 20, 期 22, 页码 7158-7162出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.8b03098
关键词
-
资金
- National Natural Science Foundation of China [21572110, 21372137, 21607164, 21801152]
An efficient synthesis of thiazolidine-2,4,5-triimine derivatives was developed via Ni-catalyzed oxidative double isocyanide insertion to thioureas under air conditions, in which thioureas play three roles as a substrate, a ligand, and overcoming isocyanide polymerization. The reaction is featured by employing a low-cost and low loading Ni(acac)(2) catalyst, without any additives, and high atom economy. This is the first example to directly apply a Ni(II) catalyst in oxidative double isocyanide insertion reactions.
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