期刊
ORGANIC LETTERS
卷 20, 期 22, 页码 7257-7260出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.8b03170
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资金
- Natural Sciences and Engineering Research Council of Canada
- Fonds de recherche du Quebec-Nature et technologies
- Universite Laval
The synthesis of 5-[(pentafluorosulfanyl)methyl]-2-oxazolines is reported. The use of a silver promoter allows the intramolecular cyclization of N-[2-chloro-3-(pentafluorosulfanyl)propyl] amide to occur without elimination of the chlorine atom, a reaction pathway typically observed for beta-chloro-SF5-alkyl compounds. The products, potentially valuable SF5-containing heterocycles, are obtained in up to 97% yield.
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