期刊
LETTERS IN ORGANIC CHEMISTRY
卷 16, 期 11, 页码 911-914出版社
BENTHAM SCIENCE PUBL LTD
DOI: 10.2174/1570178616666181203142445
关键词
Diacetoxyiodoarenes; acetic anhydride; sodium perborate; intramolecular rearrangement; ideal yields; iodoarenes
资金
- Henan Provincial Science and Technology Department Project [172102310436]
- Henan Polytechnic University Medical Special Fund [NSFRF1622, NSFRF170701]
This study introduces a concise and efficient method for preparing diacetoxyiodoarenes from the corresponding iodoarenes. In the presence of acetic anhydride, iodoarenes were oxidized to diacetoxyiodoarenes by sodium perborate in acetic acid under argon protection at 55 degrees C in ideal yields. Through this method, 10 diacetoxyiodoarenes were obtained smoothly.
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