期刊
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY
卷 141, 期 2, 页码 805-809出版社
AMER CHEMICAL SOC
DOI: 10.1021/jacs.8b12185
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- MPG
The constrained tricyclic skeleton of the nor-cembranoid sinulariadiolide (1) with a nine-membered nexus was obtained by a cascade of transannular Michael reaction, carbonate elimination, butenolide formation, and spontaneous oxa-Michael addition of MeOH. The required macrocyclic precursor was prepared by ring-closing alkyne metathesis followed by trans-hydrostannation/carbonylation.
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