期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 84, 期 2, 页码 1064-1069出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.8b02670
关键词
-
资金
- National Natural Science Foundation of China [21562025]
An unprecedented method for cleaving the C=C bond in N,N-disubstituted enaminones in the presence of elemental sulfur and N,N-dimethyl-4-aminopyridine is disclosed. Without using any metal catalyst or additive, the cascade functionalization of both C=C and C-H bonds takes place to enable the formation of new C=S and C-N bonds, thus providing a facile and practical method for the synthesis of N,N-disubstituted alpha-keto thioamides.
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