期刊
JOURNAL OF MAGNETISM AND MAGNETIC MATERIALS
卷 469, 期 -, 页码 467-482出版社
ELSEVIER
DOI: 10.1016/j.jmmm.2018.09.002
关键词
Nanocrystalline equiatomic NiCoFe alloy; Mechanical alloying; Lattice parameter; Saturation magnetization; Intrinsic coercivity
资金
- Institute of Advanced Vehicle Systems at the University of Michigan in Dearborn [U052349]
- College of Engineering and Computer Science
Mechanically alloying equiatomic Ni, Co, and Fe powder blends for 9 h resulted in the formation of nanocrystalline equiatomic NiCoFe alloy powders comprised of. gamma-phase. The crystallite size and the lattice parameter was similar to 20 +/- 5 nm and 0.3597 +/- 0.0005 nm, respectively. The mode of the powders was 3-7 mu m. The saturation magnetization (M-S) and the intrinsic coercivity (H-CI) of the alloy, at 300 K, was similar to 136 +/- 5 Am-2/kg and similar to 2.0 +/- 0.2 kA/m, respectively. Both M-S and H-CI, irrespective of the milling media and milling atmosphere, decreased with increase in temperature from 60 K to 300 K. At elevated temperatures (400 K to 880 K), the alloy powders maintained the gamma-phase up to 640 K, thereafter it was comprised of gamma-phase and alpha-Fe. In the temperature regime 300-640 K, the percentage decrease in M-S and H-CI was similar to 12% and similar to 30%, respectively. The M-S and H-CI at 300 K, after the magnetization versus applied magnetic field (M-H) run at 640 K, was similar to 136 Am-2/kg and similar to 1.5 kA/m, respectively; while the same after the M-H run at 880 K was similar to 154 Am-2/kg and similar to 1.0 kA/m, respectively. Annealing of the nanocrystalline alloy powders is likely to improve its soft-magnetic properties.
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