期刊
CHEMICAL AND BIOCHEMICAL ENGINEERING QUARTERLY
卷 32, 期 3, 页码 315-324出版社
CROATIAN SOC CHEMICAL ENGINEERING TECHNOLOGY
DOI: 10.15255/CABEQ.2017.1146
关键词
deep eutectic solvents; Ginkgo biloba; Ginkgo flavonoids; extraction; recovery
资金
- China Postdoctoral Science Foundation [2016M600417, 2017T100373]
- 333 project of Jiangsu Province [BRA2017458]
- Six Talent Peaks Project in Jiangsu Province [2015-JY-016]
- Open Project of State Key Laboratory of Natural Medicines [SKLNMKF201802]
- Priority Academic Program Development of Jiangsu Higher Education Institutions, PAPD
Deep eutectic solvent (DES)/water mixture as alternative extraction solvent was proposed for the efficient extraction of Ginkgo flavonoids from Ginkgo biloba leaves. Fifty DESs were prepared and investigated for the extraction of Ginkgo flavonoids. Compared with the present most efficient extraction solvent (70 % ethanol in water), three DESs, choline chloride/1,3-butanediol (ChCl/B), choline chloride/levulinic acid (ChCl/LA1), and 1,2-propanediol/levulinic acid (P/LA1), gave obviously higher extraction yields. The extraction process was further optimized systematically. The optimized extraction conditions were as follows: ChCl/LA1 containing 40 % (w/w) water was used as the solvent to extract Ginkgo flavonoids at a solvent to solid ratio of 10:1 (v/w) with stirring at 50 degrees C and 150 rpm for 15 min. Under the optimal conditions, 99.87 % of Ginkgo flavonoids could be extracted from the Ginkgo biloba leaves powder at a time. Furthermore, the recovery of Ginkgo flavonoids in the DES extraction solution was efficiently achieved using macroporous resin AB-8, which gave a recovery yield of 93.7 %. The DES-based extraction combined with macroporous resin recovery developed in this work can be an efficient alternative method for the extraction and separation of Ginkgo flavonoids from Ginkgo biloba leaves.
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