期刊
ANALYTICAL AND BIOANALYTICAL CHEMISTRY
卷 411, 期 9, 页码 1863-1871出版社
SPRINGER HEIDELBERG
DOI: 10.1007/s00216-018-1521-9
关键词
Carbon nanodots; Surface-enhanced infrared absorption spectroscopy; SEIRA; Attenuated total reflection; ATR; Adenine
资金
- Chinese Scholarship Council (CSC)
- DAAD U5-Ulm University [57271317]
- Startup Funding of Distinguished Professorship of 1000 Talents Program [31370086963030]
In this study, carbon nanodots (CNDs) with excellent aqueous dispersibility, narrow size distribution, and oxygen-rich functional groups have been prepared via a green electrochemical method. Graphite electrodes were directly electrolyzed at ambient temperatures to form uniform CNDs in deionized water, which is free from additional oxidant/reductant. As-synthesized CNDs have been applied to coat an attenuated total reflection (ATR) waveguide enabling surface-enhanced infrared absorption (SEIRA) spectroscopic studies for detecting a variety of analytes in aqueous phase with remarkably enhanced IR band intensities. Finally, the proposed ATR-SEIRA strategy enabled quantitatively analyzing adenine in aqueous solution after optimizing the amount of CNDs, the solution pH, and potential CND aggregation.
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