期刊
ORGANIC CHEMISTRY FRONTIERS
卷 5, 期 18, 页码 2652-2656出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c8qo00740c
关键词
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资金
- Science and Technology Planning Project of Guangdong Province [2015A020211026, 2017A010103044]
- 100 Young Talents Programme of Guangdong University of Technology [220413506]
- Open Fund of the Key Laboratory of Functional Molecular Engineering of Guangdong Province (South China University of Technology) [2016kf07]
A convenient and efficient C(sp(3))-H phosphorylation has been achieved via the metal-free DDQ-mediated cross-dehydrogenative coupling between diarylphosphine oxides and xanthene derivatives at room temperature. This transformation provides a direct synthetic route to the construction of C(sp(3))-P bonds with good functional group compatibility, leading to the formation of alkylphosphonates in up to 96% yield.
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