期刊
ORGANIC CHEMISTRY FRONTIERS
卷 1, 期 7, 页码 821-824出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c4qo00089g
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资金
- Engineering and Physical Sciences Research Council [EP/K039687/1] Funding Source: researchfish
- EPSRC [EP/K039687/1] Funding Source: UKRI
We describe a practical, economical, and scalable multi-gram synthesis of 1-vinylcyclopropyl 4-methyl-benzenesulfonate. This intermediate is important for the rapid and economical synthesis of alkylidenecyclopropanes, which provides access to a variety of alicyclic systems via metal-catalysed higher-order carbocyclization and cycloisomerization reactions.
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