4.2 Article

Characterization of an in-vacuum PILATUS 1M detector

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JOURNAL OF SYNCHROTRON RADIATION
卷 21, 期 -, 页码 529-536

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INT UNION CRYSTALLOGRAPHY
DOI: 10.1107/S160057751400294X

关键词

hybrid pixel detector; PILATUS detector; solid-state detectors; detector design; small-angle X-ray scattering; SAXS; ASAXS; GISAXS; nanometrology; detector quantum efficiency

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A dedicated in-vacuum X-ray detector based on the hybrid pixel PILATUS 1M detector has been installed at the four-crystal monochromator beamline of the PTB at the electron storage ring BESSY II in Berlin, Germany. Owing to its windowless operation, the detector can be used in the entire photon energy range of the beamline from 10 keV down to 1.75 keV for small-angle X-ray scattering (SAXS) experiments and anomalous SAXS at absorption edges of light elements. The radiometric and geometric properties of the detector such as quantum efficiency, pixel pitch and module alignment have been determined with low uncertainties. The first grazing-incidence SAXS results demonstrate the superior resolution in momentum transfer achievable at low photon energies.

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