期刊
JOURNAL OF MATERIALS CHEMISTRY A
卷 2, 期 48, 页码 20612-20620出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c4ta04054f
关键词
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资金
- EPSRC [EP/K039547/1]
- EPSRC-funded Leeds EPSRC Nanoscience and Nanotechnology Equipment Facility (LENNF) [EP/K023853/1]
- Engineering and Physical Sciences Research Council [EP/K023853/1, EP/K039547/1] Funding Source: researchfish
- EPSRC [EP/K023853/1, EP/K039547/1] Funding Source: UKRI
Iron selenide nanocrystals (NCs) were synthesised by the thermolysis of single molecular precursors, bis(tetraisopropyldiselenoimidodiphosphinato)iron(II) (3) and bis(tetraphenyldiselenoimidodiphosphinato)iron(II) (4) in oleylamine and hexadecylamine at different growth temperatures. TEM images of the NCs showed the rod and plate-like crystallites. Both complexes were also used for the deposition of thin films by Aerosol Assisted Chemical Vapour Deposition (AACVD) onto silicon substrates. SEM images of thin films deposited from complex (3) and (4) showed significantly different morphologies under similar conditions. X-ray single crystal structures of complexes [Fe{(SePPh2)(2)N}(2)] (4) and [(SePPh2)(2)N)-O-(SePPh2)(2)N)] (5) were also determined.
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