期刊
ACS MACRO LETTERS
卷 1, 期 8, 页码 1051-1055出版社
AMER CHEMICAL SOC
DOI: 10.1021/mz300349z
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资金
- German Research Foundation (DFG)
- Netherland Organization for Scientific Research (NWO)
The investigation of poly(butylene-2,6-naphthalate) crystallization by means of chip-calorimetry and ultrafast wide-angle X-ray diffraction (WAXD) revealed the existence of two possible mechanisms. The formation Of the stable triclinic-alpha-phase occurs directly from the undercooled melt at law cooling rates/high crystallization temperature. At higher cooling rates a two-stage route is observed: crystallization is preceded by the formation of a mesomorphic phase from the isotropic melt The monotiopic behavior of poly(butylene-2,6-naphthalate), becoming apparent only under severe cooling conditions, obeys the well-known Ostwald's rule of stages.
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