期刊
SCIENTIFIC REPORTS
卷 6, 期 -, 页码 -出版社
NATURE PUBLISHING GROUP
DOI: 10.1038/srep36316
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资金
- College of Science and Mathematics, Arkansas State University, Jonesboro
- National Institute of General Medical Sciences of the National Institutes of Health (NIH) [P30 GM103450]
- National Institutes of Health (NIH) National Institute of General Medical Sciences (NIGMS) [P20 GM103429]
- Saudi Arabian Cultural Mission (SACM)
- National Science Foundation-EPSCoR [EPS-0701890]
An efficient synthesis of novel 2,3-dihydro-4H-pyrido[1,2-a] pyrimidin-4-ones has been reported. Inexpensive and readily available substrates, environmentally benign reaction condition, and product formation up to quantitative yield are the key features of this methodology. Products are formed by the aza-Michael addition followed by intramolecular acyl substitution in a domino process. The polar nature and strong hydrogen bond donor capability of 1,1,1,3,3,3-hexafluoropropan-2-ol is pivotal in this cascade protocol.
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