期刊
RSC ADVANCES
卷 3, 期 44, 页码 22280-22284出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c3ra44484h
关键词
-
资金
- National Natural Science Foundation of China [21171133, 21271143]
We have developed a catalyst-free system for the 3-sulfenylation of free (N-H) indoles using mercaptobenzoic acid under alkaline conditions. The use of this system provides a green, convenient, and efficient method for the synthesis of 3-sulfenylindoles in good yields and with high selectivity. This simple synthesis process was carried out in a green solvent, isopropanol/H2O, under atmospheric and catalyst-free conditions. The procedure is suitable for use with N-unprotected indoles.
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