4.6 Article

Synthesis of gamma-valerolactone using a continuous-flow reactor

期刊

RSC ADVANCES
卷 3, 期 37, 页码 16283-16287

出版社

ROYAL SOC CHEMISTRY
DOI: 10.1039/c3ra43032d

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资金

  1. Hungarian National Scientific Research Fund [OTKA-CNK 78065]
  2. European Union
  3. European Social Fund under the Social Renewal Operational Programme (SROP) [TAMOP-422B10-1-2010-0009]

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This study describes the heterogeneous catalysed continuous synthesis of gamma-valerolactone (GVL) using a continuous-flow reactor, H-Cube (R) and H-Cube Pro (TM), equipped with 5% Ru/C, 10% Pd/C and RANEY (R) Ni CatCart (R). The highest yield of GVL was achieved by using 5% Ru/C in the presence of 0.015 mol L-1 Bu-P(C6H4-m-SO3Na)(2) ligand under 100 bar H-2 at 100 degrees C.

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