期刊
CATALYSIS SCIENCE & TECHNOLOGY
卷 4, 期 9, 页码 3235-3243出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c4cy00411f
关键词
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资金
- National Natural Science Foundation of China [21373069]
- New Century Excellent Talents in University [NCET-10-0064]
- State Key Lab of Urban Water Resource and Environment of Harbin Institute of Technology [HIT2013TS01]
- Fundamental Research Funds for the Central Universities [HIT. IBRSEM. 201327]
A low-cost, widely available and environmentally benign compound guanidine hydrochloride was applied to prepare g-C3N4 by thermal-induced polymerization at different temperatures. The as-prepared g-C3N4 was thoroughly characterized by X-ray diffraction, Fourier transform infrared spectroscopy, elemental analyses, N-2 adsorption-desorption isotherms, thermal gravimetric analysis and differential scanning calorimetry, transmission electron microscopy, UV-vis diffuse reflectance spectra and photoluminescence spectra. It was noticeable that g-C3N4 prepared from guanidine hydrochloride possessed a much larger surface area than that prepared from melamine. And its photocatalytic activity was evaluated for degrading Rhodamine B dye which demonstrated that the g-C3N4 synthesized from guanidine hydrochloride exhibited a much higher activity than that prepared from melamine. Moreover, the activity can be further enhanced by increasing the condensation temperature of g-C3N4. In addition, the as-prepared g-C3N4 was also stable as demonstrated in the recycling experiments.
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