期刊
BEILSTEIN JOURNAL OF NANOTECHNOLOGY
卷 4, 期 -, 页码 285-291出版社
BEILSTEIN-INSTITUT
DOI: 10.3762/bjnano.4.31
关键词
continuous parallel analysis; ESI-MS; 3D printing; reactionware; supramolecular chemistry
资金
- EPSRC
- Royal Society/Wolfson Foundation
- Leverhulme Trust
- University of Glasgow
- WestCHEM
- EPSRC [EP/F016360/1] Funding Source: UKRI
- Engineering and Physical Sciences Research Council [EP/F016360/1] Funding Source: researchfish
Herein, we present an approach for the rapid, straightforward and economical preparation of a tailored reactor device using three-dimensional (3D) printing, which can be directly linked to a high-resolution electrospray ionisation mass spectrometer (ESI-MS) for real-time, in-line observations. To highlight the potential of the setup, supramolecular coordination chemistry was carried out in the device, with the product of the reactions being recorded continuously and in parallel by ESI-MS. Utilising in-house-programmed computer control, the reactant flow rates and order were carefully controlled and varied, with the changes in the pump inlets being mirrored by the recorded ESI-MS spectra.
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