期刊
ACS COMBINATORIAL SCIENCE
卷 13, 期 1, 页码 2-6出版社
AMER CHEMICAL SOC
DOI: 10.1021/co100015b
关键词
hydrazones; microwave synthesis; cooling while heating; open vessel
资金
- Ministero dell'Universita e della Ricerca [200879X9N9]
- Istituto Pasteur
- Fondazione Cenci Bolognetti [2009]
- FILAS (Finanziaria Laziale di Sviluppo) [2010]
We reported the first example of open vessel and cooling while heating microwave-assisted synthesis of pyridinyl N-aryl hydrazones. Compounds were prepared in excellent isolated yields (88-98%) in only 5 min, by reacting 4- and 2,4-(di) substituted phenylhydrazines, bearing both electron-donating (4-CH3, 4-OCH3) and -withdrawing (4-Cl, 4-Br, 4CF(3), 4-NO2, 2,4-Cl-2) groups with 2-, 3-, and 4-acetylpyridine. The method was successfully extended to other carbonyl compounds.
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