期刊
ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE
卷 636, 期 11, 页码 1917-1919出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/zaac.201000222
关键词
Lithium; Zinc; Structure elucidation; Thermal properties; Intermetallic phases
By simultaneous deposition of zinc and lithium onto a cooled sapphire substrate, LiZn13 was obtained for the first time. It crystallizes in the NaZn13 structure type (Fm (3) over bar, a = 1234.92(6) pm, R-p = 5.4 %, R-wp = 6.9 %, structure analysis with the Rietveld-method). Single-phase LiZn13 forms from a hexagonal Li0.07Zn0.93 alloy, deposited at -196 degrees C, during heating up to room temperature. Above room temperature LiZn13 decomposes.
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