期刊
ULTRASONICS SONOCHEMISTRY
卷 18, 期 2, 页码 489-493出版社
ELSEVIER SCIENCE BV
DOI: 10.1016/j.ultsonch.2010.10.003
关键词
Ultrasound-assisted synthesis; Response surface methodology; Central composite design; O-allylation; Allyl 1-naphthyl ether
Allyl 1-naphthyl ethers are useful compounds for different purposes, but reported methods to synthesize them require long reaction times. In this work, we have obtained allyl 1-naphthyl ether in good yield using ultrasonic-assisted methodology in a 1-h reaction. A central composite design was used to obtain a statistical model and a response surface (p < 0.05; R-2 = 0.970; R-adj(2) = 0.949; R-pred(2) = 0.818) that can predict the optimal conditions to maximize the yield, validated experimentally. (C) 2010 Elsevier B.V. All rights reserved.
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