期刊
ASIAN JOURNAL OF ORGANIC CHEMISTRY
卷 4, 期 6, 页码 521-524出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ajoc.201500063
关键词
anilines; diazotization; palladium; silver nitrite; Suzuki reaction
资金
- GSK-Singapore partnership for green and sustainable manufacturing (GSM)
- Institute of Chemical and Engineering Sciences
A Pd-catalyzed, convenient, and simple one-pot method for the preparation of unsymmetrical biaryls from anilines is established via an insitu diazotization reaction using silver nitrite (AgONO) as an alternative nitrosating reagent. The protocol works under ligand- and base-free conditions at room temperature and tolerates a variety of functionalized anilines and arylboronic acids leading to the corresponding biaryl products in moderate to good yields.
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