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Novel carbohydrate-derived pyridinecarboxylic organocatalysts for the enantioselective reduction of imines with trichlorosilane

期刊

TETRAHEDRON-ASYMMETRY
卷 25, 期 8, 页码 596-601

出版社

PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetasy.2014.03.015

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资金

  1. Natural Science Foundation of China [21376213]
  2. Research Fund for the Doctoral Program of Higher Education of China [20120101110062]
  3. Low Carbon Fatty Amine Engineering Research Center of Zheijiang Province [2012E10033]

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A new type of carbohydrate-derived pyridinecarboxylic organocatalyst was prepared by fine-tuning a D-glucosamine backbone at the C-2 and C-3 positions. The carbohydrate-derived pyridinecarboxylic organocatalyst was used for the enantioselective reduction of imines with trichlorosilane. The reduction proceeded in high yield (up to 93%) and with moderate enantioselectivity (up to 75%). (C) 2014 Elsevier Ltd. All rights reserved.

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