期刊
TETRAHEDRON-ASYMMETRY
卷 23, 期 2, 页码 117-123出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetasy.2012.01.014
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资金
- MOES
- CSIR-UGC, New Delhi, India
A simple and efficient stereoselective synthesis of clonostachydiol was achieved using ethyl (R)-3-hydroxybutanoate 5 and methyl (R)-2-hydroxypropanoate 12 as readily available starting materials. The key steps involved in the synthesis were MacMillan alpha-hydroxylation, Horner-Wadsworth-Emmons (HWE) olefination, a Grignard reaction, and Hoveyda-Grubbs IInd generation catalyzed ring closing metathesis (RCM). (C) 2012 Elsevier Ltd. All rights reserved.
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