4.4 Article

Tandem oxidative amidation of benzyl alcohols with amine hydrochloride salts catalysed by iron nitrate

期刊

TETRAHEDRON LETTERS
卷 54, 期 36, 页码 4922-4925

出版社

PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2013.07.005

关键词

Oxidative amidation; Benzyl alcohol; Amides; Iron(III) nitrate; Tandem oxidation

资金

  1. GlaxoSmithKline (GSK)
  2. Singapore Economic Development Board (EDB) for Green and Sustainable Manufacturing (GSM)
  3. Agency for Science, Technology and Research (A*STAR), Singapore

向作者/读者索取更多资源

A tandem process for the oxidative amidation of benzyl alcohols with amine hydrochloride salts has been developed using inexpensive Fe(NO3)(3) as the catalyst, air and aqueous t-butyl hydroperoxide as oxidants. A wide range of benzamides have been synthesized under mild conditions. This greener amide formation method provides an economical and practical assess to benzamides from readily available and inexpensive starting materials. (C) 2013 Elsevier Ltd. All rights reserved.

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