期刊
TETRAHEDRON LETTERS
卷 54, 期 49, 页码 6679-6681出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2013.09.016
关键词
Unsaturated amides; Synthesis; Copper; Catalysis; Oxidative coupling
资金
- National Natural Science Foundation of China [21074054, 21172106]
- National Basic Research Program of China [2010CB923303]
- Research Fund for the Doctoral Program of Higher Education of China [20120091110010]
A novel and efficient protocol for the synthesis of alpha,beta-unsaturated amides has been developed using catalytic amount of Cu(OAc)(2) and TBHP as an available oxidant. Oxidative coupling of various unsaturated carboxylic acids with N,N-disubstituted formamides was examined to furnish the desired products in good yields. (C) 2013 Elsevier Ltd. All rights reserved.
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