期刊
TETRAHEDRON LETTERS
卷 53, 期 45, 页码 6067-6070出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2012.08.134
关键词
Hydrogen bonding; Pseudopolymorphism; Tricyclohexane triperoxide; Single crystal XRD; Thermal stability
资金
- University of Delhi
- University Scientific Instrumentation Center (USIC), University of Delhi, Delhi, India
- UGC
Tricyclohexane triperoxide (TCTP) was synthesized as a main by-product of tetraoxane synthesis and was characterized by spectroscopic techniques viz. H-1 NMR, C-13 NMR, FT-IR and Raman. The single crystal X-ray structure revealed the inclusion of solvent in 1:1 stoichiometric ratio involving a unique trifurcated C(sp(3))-H center dot center dot center dot O hydrogen bonding imparting remarkable symmetry to the molecule. The thermal stability of single crystal was determined by TG-DTA and DSC. (C) 2012 Elsevier Ltd. All rights reserved.
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