期刊
TETRAHEDRON LETTERS
卷 53, 期 16, 页码 2078-2081出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2012.02.035
关键词
Palladium; Phosphinylthiolation; Alkyne; Homogeneous catalysis
资金
- MEXT, Japan [18065008]
- Grants-in-Aid for Scientific Research [18065008] Funding Source: KAKEN
Phosphinylthiolation of terminal alkynes with Ph2P(O)SBu or a related compound proceeds in the presence of a palladium-PEt3 catalyst system. Activity and stereoselectivity are highly dependent on the nature of solvent, ethylbenzene, and n-hexanol (or t-amyl alcohol) being E- and Z-selective, respectively. (C) 2012 Elsevier Ltd. All rights reserved.
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