期刊
TETRAHEDRON LETTERS
卷 53, 期 13, 页码 1553-1557出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2012.01.015
关键词
Oxazole; Coumarin; Quinolone; Pyridine; Cs2CO3; DMSO
资金
- CSIR (New Delhi)
- DST (New Delhi)
An efficient approach for the synthesis of coumarin-, quinolone- and pyridine-annulated oxazole derivatives has been achieved by direct base-mediated intramolecular carbon-oxygen bond formation in a transition metal catalyst-free protocol. Intramolecular cyclization of o-bromoamides in DMSO in the presence of Cs2CO3 at 130 degrees C affords heterocycle-annulated oxazole derivatives in high yields via a nucleophilic ;addition of amide to form the C-O bond. (C) 2012 Published by Elsevier Ltd.
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