期刊
TETRAHEDRON LETTERS
卷 53, 期 32, 页码 4077-4079出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2012.05.110
关键词
(-)-Enniatin B; Macrolactamization; Cyclic hexadepsipeptide; Ammonium ionophore; Precipitation-free
资金
- Winston Churchill Foundation
- BP Endowment
- Georganics Ltd
- Industrieclub Dusseldorf
A nine-step (longest linear) batch total synthesis of the cyclic hexadepsipeptide (-)-enniatin B is described. The synthesis minimizes precipitation during reaction conditions for adaptability to flow synthesis. The route was used to prepare >100 mg of the natural product. Crown Copyright (C) 2012 Published by Elsevier Ltd. All rights reserved.
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