期刊
TETRAHEDRON LETTERS
卷 52, 期 12, 页码 1339-1342出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2011.01.076
关键词
Indoles; Nitrocinnamates; Nitrostyrenes; Phosphines; Microwaves
资金
- Science and Engineering Research Council of A*STAR (Agency for Science, Technology and Research), Singapore
A concise, efficient and simple route to a series of bromoindole building blocks is described. The synthetic routes are highlighted by purification-free preparation of o-nitrocinnamate intermediates and clean, modified Cadogan indole syntheses. The scope of this indole synthesis has been explored and expanded through the use of a range of solvents and easily removable phosphine reagents. (C) 2011 Elsevier Ltd. All rights reserved.
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