期刊
TETRAHEDRON LETTERS
卷 51, 期 3, 页码 537-539出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2009.11.085
关键词
-
资金
- Donors of the Petroleum Research Fund
- American Chemical Society
- Wyeth
An efficient synthesis of lycogarubin C (3) was completed in seven steps from the known 1-(phenylsulfonyl)indole-3-carbaldehyde in 30% overall yield, via a Diels-Alder reaction between (Z)-1,2-di(1H-indol-3-yl)ethene 9b and dimethyl 1,2,4,5-tetrazine-3,6-dicarboxylate (7), followed by a Kornfeld-Boger ring contraction to form the pyrrole ring. (C) 2009 Elsevier Ltd. All rights reserved.
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