期刊
TETRAHEDRON LETTERS
卷 50, 期 52, 页码 7327-7329出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2009.10.049
关键词
2-Deoxyglycosides; Microwave-assisted glycosylation; alpha-2-Deoxy-ulosides; Michael-type additions
资金
- National Science Council of Taiwan [NSC96-2113-M-039-002]
- China Medical University, Taiwan [CMU96-139, CMU97-226]
alpha-2-Deoxyglycosides were successfully synthesized by means of microwave-assisted glycosylation. Hex-1-en-3-uloses were treated with a catalytic amount of AlCl3 and various O-nucleophiles including alcohols and sugars under microwave conditions. The desired alpha-2-deoxy-ulosides products were obtained in good to excellent yields with high stereoselectivity (alpha/beta >= 88/12). Crown Copyright (C) 2009 Published by Elsevier Ltd. All rights reserved.
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