期刊
TETRAHEDRON LETTERS
卷 50, 期 37, 页码 5280-5282出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2009.07.014
关键词
Ethenolysis; 2nd-generation Hoveyda-Grubbs catalyst; Absolute configuration; J-based configuration analysis
资金
- JSPS [16GS0206]
- Ministry of Education, Science, Sports and Culture, Japan
- Grants-in-Aid for Scientific Research [16GS0206, 21651091] Funding Source: KAKEN
The degradation product C14-C23 2 was obtained using ethenolysis with the 2nd-generation Hoveyda-Grubbs catalyst from 62-membered lactone in symbiodinolide (1). The absolute configurations of three chiral centers in fragment 2 were assigned as 17R, 18R, and 21R by a combination of J-based configuration analysis and the Mosher-Riguera method. (c) 2009 Elsevier Ltd. All rights reserved.
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