期刊
TETRAHEDRON LETTERS
卷 50, 期 11, 页码 1226-1228出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2009.01.009
关键词
(o-Silylphenyl)lithium; Bis(o-silylphenyl)cuprate; Oxidative coupling; Bipheny
资金
- Ministry of Education, Culture, Sports, Science and Technology, Japan [19020048]
- Grants-in-Aid for Scientific Research [19020048] Funding Source: KAKEN
Bis[o-(hydrosilyl)phenyl]cuprates and bis[o-(fluorosilyl)phenylicuprates were prepared by reacting [o-(hydrosilyl)phenyl]lithiums and [o-(fluorosilyl)phenyl]lithiums, respectively, with copper salts, such as CuCN and Cu(OPiv)(2). The phenylcuprates underwent oxidative coupling to afford 2,2'-bis(hydrosilyl)biphenyls and 2,2'-bis(fluorosilyl)biphenyls. (C) 2009 Elsevier Ltd. All rights reserved.
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