期刊
TETRAHEDRON LETTERS
卷 50, 期 23, 页码 2815-2817出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2009.03.169
关键词
Titanium superoxide; N-Bromosuccinimide; p-Toluenesulfonamide; Bromoamination; anti-Markovnikov addition
资金
- Department of Science and Technology, New Delhi [SR/S1/OC-72/2006]
A new facile procedure for the aminobromination of olefins in high yields has been described using p-toluene sulfonamide (p-TsNH2) and N-bromosuccinimide (NBS) as introgen and bromine sources, respectively, and titanium superoxide as a truly heterogeneous catalyst. The formation of anti-Markovnikov product exclusively in all the cases studied possibly proceeding I free radical reaction pathway is remarkable. (C) 2009 Elsevier Ltd. All rights reserved.
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