期刊
TETRAHEDRON LETTERS
卷 50, 期 26, 页码 3661-3664出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2009.03.115
关键词
-
资金
- EPSRC [GR/S25456]
- BBSRC [BB/D524140]
- SPARC
A rapid and efficient method for C-S bond formation under microwave irradiation is reported. The reaction of both electron-rich and electron-poor aryl halides with thiols using copper(I) iodide as a catalyst is facilitated by the addition of 2 equiv of trans-cyclohexane-1,2-diol as ligand in the presence Of K(2)CO(3) as base in 2-propanol. Microwave irradiation at 120 degrees C for 3 h gives the corresponding aryl sulfide in a procedure amenable to library production. (C) 2009 Elsevier Ltd. All rights reserved.
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