期刊
TETRAHEDRON
卷 68, 期 31, 页码 6186-6192出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2012.05.071
关键词
Total synthesis; Eudistomidins G, H, and I; Eudistoma glaucus; Absolute configuration
资金
- Ministry of Education, Science, Sports, and Culture of Japan
Asymmetric first total synthesis of eudistomidins G, H. and I, tetrahydro-beta-carboline alkaloids from the Okinawan marine tunicate Eudistoma glaucus, has been accomplished with the Bischler-Napieralski reaction and the Noyori catalytic asymmetric hydrogen-transfer reaction. The absolute configurations of eudistomidins G, H, and! were confirmed from comparison of the H-1 and C-13 NMR, and CD spectral data of synthetic and natural eudistomidins G, H, and I, respectively. (C) 2012 Elsevier Ltd. All rights reserved.
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